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              藥物詳細合成路線

              Name Etodolic acid;Etodolac;RAK-591;AY-24236;Lodine SR;Lodine XL;Osteluc;Hypen;Edolan;Ultradol;Lodine
              Chemical Name 1,8-Diethyl-1,3,4,9-tetrahydropyrano[3,4-b]indole-1-acetic acid
              CAS 41340-25-4
              Related CAS
              Formula C17H21NO3
              Structure
              Formula Weight 287.36182
              Stage 上市-1985
              Company Roberts (Proprietary), Wyeth Pharmaceuticals (Originator), Nippon Shinyaku (Licensee)
              Activity/Mechanism Antiarthritic Drugs, Osteoarthritis, Treatment of, Rheumatoid Arthritis, Treatment of, TREATMENT OF MUSCULOSKELETAL & CONNECTIVE TISSUE DISEASES, Cyclooxygenase-2 Inhibitors, Non-Steroidal Antiinflammatory Drugs
              Syn. Route 1
              Route 1
              by condensation of 3-(2-hydroxyethyl)-8-ethylindole (i) with ethyl 3-oxopentanoate (ii) in benzene by means of p-toluenesulfonic acid.
              List of intermediates No.
              (1s,2e)-4-[(2r,4ar,6r,8as)-6-[(2s,5r)-5-bromo-2,6,6-trimethyltetrahydro-2h-pyran-2-yl]-8a-methyloctahydropyrano[3,2-b]pyran-2-yl]-1-[(2r,5r)-5-[1-(acetoxy)-1-methylethyl]-2-methyltetrahydro-2-furanyl]-4-oxo-2-butenyl acetate (i)
              (1s)-4-[(2r,4ar,6r,8as)-6-[(2s,5r)-5-bromo-2,6,6-trimethyltetrahydro-2h-pyran-2-yl]-8a-methyloctahydropyrano[3,2-b]pyran-2-yl]-1-[(2r,5r)-5-[1-(acetoxy)-1-methylethyl]-2-methyltetrahydro-2-furanyl]-4-oxobutyl acetate (ii)
              Reference 1:
                  demerson, c.a.; et al.; 1-carboxamido pyrano(thiopyrano) [3,4-6]indole derivatives. de 2226340; fr 2140154; gb 1391005; us 3843681 .
              Reference 2:
                  castaner, j.; arrigoni-martelli, e.; etodolic acid. drugs fut 1977, 2, 1, 21.

              來源:藥化網

              作者:藥化小編

              摘要:本文合成路線介紹的是藥物中文名依托度酸;英文名Etodolic acid;Etodolac;RAK-591;AY-24236;Lodine SR;Lodine XL;Osteluc;Hypen;Edolan;Ultradol;Lodine;CAS[41340-25-4]

               
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